(E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

Base Information

Chemical Name:(E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine
CAS No.:168414-39-9
Molecular Formula:C₂₇H₃₆BrNOSi
Molecular Weight:498.578
Hs Code.:

Synonyms:(E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

Suppliers and Price of (E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

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Technology Process of (E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

There total 4 articles about (E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91239-98-4
3-[(ethylamino)methyl]phenol

: 168414-39-9
(E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / potassium carboante / dimethylsulfoxide / 6 h / 50 °C

2: 1.) palladium diacetate, copper iodide, triphenylphosphine, 2.) butylamine / 1.) THF, 1.5 h, 2.) THF, RT, 24 h

3: 1.) potassium carbonate, 2.) potassium iodide / 1.) DMSO, 90 deg C, 30 min, 2.) DMSO, 90 deg C, 5 h

With copper(l) iodide; palladium diacetate; potassium carbonate; N-butylamine; triphenylphosphine; potassium iodide; In dimethyl sulfoxide;
DOI:10.1021/jm00017a004

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 168414-39-9
(E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 3 Angstroem molecular sieves, 2.) NaBH₄ / 1.) ethanol, RT, 20 h, 2.) ethanol, 2 h

2: 75 percent / potassium carboante / dimethylsulfoxide / 6 h / 50 °C

3: 1.) palladium diacetate, copper iodide, triphenylphosphine, 2.) butylamine / 1.) THF, 1.5 h, 2.) THF, RT, 24 h

4: 1.) potassium carbonate, 2.) potassium iodide / 1.) DMSO, 90 deg C, 30 min, 2.) DMSO, 90 deg C, 5 h

With sodium tetrahydroborate; copper(l) iodide; 3 A molecular sieve; palladium diacetate; potassium carbonate; N-butylamine; triphenylphosphine; potassium iodide; In dimethyl sulfoxide;
DOI:10.1021/jm00017a004

Reference yield:

: 134865-55-7
(E)-N-(3-chloropropenyl)-N-ethyl-3-hydroxybenzylamine

: 168414-39-9
(E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-<((4-bromophenyl)dimethylsilyl)methoxy>benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) palladium diacetate, copper iodide, triphenylphosphine, 2.) butylamine / 1.) THF, 1.5 h, 2.) THF, RT, 24 h

2: 1.) potassium carbonate, 2.) potassium iodide / 1.) DMSO, 90 deg C, 30 min, 2.) DMSO, 90 deg C, 5 h

With copper(l) iodide; palladium diacetate; potassium carbonate; N-butylamine; triphenylphosphine; potassium iodide;
DOI:10.1021/jm00017a004