Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

Base Information

• Chemical Name: Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside
• CAS No.: 123567-40-8
• Molecular Formula: C₃₄H₄₂O₁₁S₂
• Molecular Weight: 690.833

Synonyms:Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

Chemical Property of Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

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Technology Process of Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

There total 1 articles about Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Methyl 3-O-(3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside (121330-39-0) + p-toluenesulfonyl chloride (98-59-9) → Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside (123567-40-8)

Guidance literature:

With pyridine; at 70 ℃; for 14h;

DOI:10.1021/jo00288a074

Reference yield: 95.0%

Methyl 3-O-(3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside (123567-40-8) → Methyl 2,6-Dideoxy-3-O-(2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside (123567-42-0)

Guidance literature:

With N-Bromosuccinimide; calcium carbonate; In tetrachloromethane; water; Irradiation;

DOI:10.1021/jo00288a074

upstream raw materials:

Methyl 3-O-(3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

p-toluenesulfonyl chloride

Downstream raw materials:

Methyl 2,6-Dideoxy-3-O-(2,6-dideoxy-4-O-(p-tolylsulfonyl)-β-D-arabino-hexopyranosyl)-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

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