2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-dithiocarboxylic acid

Base Information

• Chemical Name: 2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-dithiocarboxylic acid
• CAS No.: 75823-13-1
• Molecular Formula: C₁₀H₆Cl₂N₂O₃S₂
• Molecular Weight: 337.207

Synonyms:2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-dithiocarboxylic acid

Chemical Property of 2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-dithiocarboxylic acid

Chemical Property:

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Technology Process of 2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-dithiocarboxylic acid

There total 2 articles about 2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-dithiocarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

carbon disulfide (75-15-0,12122-00-8) + 2-(2,4-dichlorophenoxymethyl)-Δ2-1,3,4-oxadiazolin-5-one (75823-08-4) → 2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ2-1,3,4-oxadiazoline-4-dithiocarboxylic acid (75823-13-1)

Guidance literature:

With ammonium hydroxide; for 2h; Ambient temperature;

Reference yield:

2-(2,4-dichlorophenoxymethyl)-Δ2-1,3,4-oxadiazolin-5-one (75823-08-4) → 2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ2-1,3,4-oxadiazoline-4-dithiocarboxylic acid (75823-13-1)

Guidance literature:

With ammonium hydroxide; 1. 2h, room temperature 2. dil. HCl;

Reference yield: 95.0%

2-(2,4-dichlorophenyoxymethyl)-5-oxo-Δ2-1,3,4-oxadiazoline-4-dithiocarboxylic acid (75823-13-1) → Bis<2-(2,4-dichlorophenoxymethyl)-5-oxo-Δ2-1,3,4-oxadiazoline-4-thiocarbonyl> disulphide (75823-17-5)

Guidance literature:

With iodine; In ethanol; for 0.25h; Heating;

upstream raw materials:

carbon disulfide

2-(2,4-dichlorophenoxymethyl)-Δ²-1,3,4-oxadiazolin-5-one

Downstream raw materials:

Bis<2-(2,4-dichlorophenoxymethyl)-5-oxo-Δ²-1,3,4-oxadiazoline-4-thiocarbonyl> disulphide

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