C₃₇H₄₁FN₃O₂P

Base Information

Chemical Name:C₃₇H₄₁FN₃O₂P
CAS No.:1601497-39-5
Molecular Formula:C₃₇H₄₁FN₃O₂P
Molecular Weight:609.724
Hs Code.:

C<sub>37</sub>H<sub>41</sub>FN<sub>3</sub>O<sub>2</sub>P

Synonyms:C₃₇H₄₁FN₃O₂P

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Chemical Property of C₃₇H₄₁FN₃O₂P

Chemical Property:

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Technology Process of C₃₇H₄₁FN₃O₂P

There total 2 articles about C₃₇H₄₁FN₃O₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₁FN₃OP

: 1896-62-4
(E)-benzalacetone

: 1601490-90-7
C₃₇H₄₁FN₃O₂P

: 1601497-39-5
C₃₇H₄₁FN₃O₂P

Guidance literature:: (E)-benzalacetone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.75h; Inert atmosphere; Cooling with acetone-dry ice;

C₂₇H₃₁FN₃OP; In tetrahydrofuran; at -78 ℃; for 30h; Overall yield = 84 %; diastereoselective reaction; Inert atmosphere; Cooling with acetone-dry ice;
DOI:10.1016/j.tetlet.2014.03.005

Reference yield:

: 1228099-26-0
C₂₀H₂₈N₃OP

: 446-52-6
2-Fluorobenzaldehyde

: 1601490-90-7
C₃₇H₄₁FN₃O₂P

: 1601497-39-5
C₃₇H₄₁FN₃O₂P

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; titanium tetrachloride / dichloromethane / 48.5 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice

2.2: 30 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice

With titanium tetrachloride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; 2.1: |Mannich Aminomethylation / 2.2: |Mannich Aminomethylation;
DOI:10.1016/j.tetlet.2014.03.005