diacetyl-mycinose

Base Information

Chemical Name:diacetyl-mycinose
CAS No.:14702-56-8
Molecular Formula:C₁₂H₂₀O₇
Molecular Weight:276.287
Hs Code.:

Synonyms:diacetyl-mycinose

Suppliers and Price of diacetyl-mycinose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diacetyl-mycinose

Chemical Property:

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Technology Process of diacetyl-mycinose

There total 3 articles about diacetyl-mycinose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338971-67-7
C₂₁H₂₆O₅

: 14702-56-8,84171-65-3,121423-37-8,22893-93-2
β-diacetyl-mycinose

: 1363813-96-0
C₁₂H₂₀O₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 20 °C

2.1: palladium 10% on activated carbon; hydrogen; acetic acid / 20 °C / ultrasound irradiation

2.2: 20 °C

With palladium 10% on activated carbon; hydrogen; sodium hydride; acetic acid; In tetrahydrofuran;
DOI:10.2174/157017811797249290

Reference yield:

: C₁₄H₂₀O₅

: 14702-56-8,84171-65-3,121423-37-8,22893-93-2
β-diacetyl-mycinose

: 1363813-96-0
C₁₂H₂₀O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / dichloromethane / Reflux

2.1: sodium hydride / tetrahydrofuran / 20 °C

3.1: palladium 10% on activated carbon; hydrogen; acetic acid / 20 °C / ultrasound irradiation

3.2: 20 °C

With palladium 10% on activated carbon; hydrogen; sodium hydride; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.2174/157017811797249290

Reference yield:

: 1338971-69-9
C₂₂H₂₈O₅

: 108-24-7
acetic anhydride

: 14702-56-8,84171-65-3,121423-37-8,22893-93-2
β-diacetyl-mycinose

: 1363813-96-0
C₁₂H₂₀O₇

Guidance literature:: C₂₂H₂₈O₅; With palladium 10% on activated carbon; hydrogen; acetic acid; at 20 ℃; ultrasound irradiation;

acetic anhydride; With pyridine; at 20 ℃;
DOI:10.2174/157017811797249290