[5-(4-Bromophenyl)furan-2-yl]methanamine hydrochloride

Base Information

• Chemical Name: [5-(4-Bromophenyl)furan-2-yl]methanamine hydrochloride
• CAS No.: 39169-94-3
• Molecular Formula: C11H10 Br N O
• Molecular Weight: 252.11
• European Community (EC) Number: 877-926-4
• DSSTox Substance ID: DTXSID80585865
• Mol file: 39169-94-3.mol

Synonyms:[5-(4-bromophenyl)furan-2-yl]methanamine hydrochloride;1049741-11-8;39169-94-3;[5-(4-bromophenyl)furan-2-yl]methanamine;hydrochloride;(5-(4-Bromophenyl)furan-2-yl)methanamine hydrochloride;DTXSID80585865;EN300-25509;G56656;Z212062932;1-[5-(4-Bromophenyl)furan-2-yl]methanamine--hydrogen chloride (1/1)

Chemical Property of [5-(4-Bromophenyl)furan-2-yl]methanamine hydrochloride

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.598
• Boiling Point: 336.6°Cat760mmHg
• Flash Point: 157.4°C
• PSA: 39.16000
• Density: 1.451g/cm³
• LogP: 4.67010
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 286.97125
• Heavy Atom Count: 15
• Complexity: 180

Purity/Quality:

99% ^*data from raw suppliers

[5-(4-BROMOPHENYL)-2-FURYL]METHYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C2=CC=C(O2)CN)Br.Cl

Technology Process of [5-(4-Bromophenyl)furan-2-yl]methanamine hydrochloride

There total 9 articles about [5-(4-Bromophenyl)furan-2-yl]methanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bromoiodobenzene (589-87-7) → (2,2-diphenylethene-1,1-diyl)bis((4-bromophenyl)selane) + (5-(4-bromophenyl)furan-2-yl)methanamine (39169-94-3) + 5-(4'-bromophenyl)furan-2-carbaldehyde oxime (39170-09-7)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate; copper(l) iodide; lithium chloride / N,N-dimethyl-formamide / 48 h / 150 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / toluene / 24 h / 50 °C / Schlenk technique; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; caesium carbonate; triethylamine; lithium chloride; In N,N-dimethyl-formamide; toluene; 1: |Ullmann Condensation / 2: |Sonogashira Cross-Coupling;

DOI:10.1002/cplu.201900213

Reference yield:

1,4-bromoiodobenzene (589-87-7) → (2,2-diphenylethene-1,1-diyl)bis((4-bromophenyl)selane) + (5-(4-bromophenyl)furan-2-yl)methanamine (39169-94-3) + 5-(4'-bromophenyl)furan-2-carbaldehyde oxime (39170-09-7) + C43H28N6S2 + 9-(4-((4-([2,2’:6’,2’’-terpyridin]-4’-yl)phenyl)ethynyl)phenyl)-9H-carbazole

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate; copper(l) iodide; lithium chloride / N,N-dimethyl-formamide / 48 h / 150 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / toluene / 24 h / 50 °C / Schlenk technique; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; caesium carbonate; triethylamine; lithium chloride; In N,N-dimethyl-formamide; toluene; 1: |Ullmann Condensation / 2: |Sonogashira Cross-Coupling;

DOI:10.1002/cplu.201900213

Reference yield:

5-(4'-bromophenyl)furan-2-carbaldehyde oxime (39170-09-7) → (5-(4-bromophenyl)furan-2-yl)methanamine (39169-94-3)

Guidance literature:

With hydrogenchloride; zinc; In ethanol; water; at 80 ℃; for 2h;

DOI:10.3390/molecules24152724

upstream raw materials:

furan-2-ylmethanamine

4-bromo-aniline

5-(4-bromophenyl)furan-2-carbonitrile

5-formylfurane-2-boronic acid

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