1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose
CAS No.:117153-32-9
Molecular Formula:C₂₁H₂₃N₃O₁₄
Molecular Weight:541.425
Hs Code.:

Synonyms:1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

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Technology Process of 1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

There total 6 articles about 1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 99-33-2
3,5-dinitrobenoyl chloride

: 117153-32-9
1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2015.06.004

Reference yield:

: 17460-45-6,23707-23-5,23739-93-7,23743-51-3,26108-75-8,59042-16-9,124516-07-0,124580-56-9
tetra-acetyl glucosamine

: 99-33-2
3,5-dinitrobenoyl chloride

: 117153-32-9
1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With pyridine;

Reference yield:

: 7597-81-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(4-methoxybenzylidene)amino-β-D-glucopyranose

: 117153-32-9
1,3,4,6-tetra-O-acetyl-2-N-(3,5-dinitro)benzoyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / acetone; water / 1 h / 0 °C

2: triethylamine / dichloromethane / 2 h / 20 °C

With hydrogenchloride; triethylamine; In dichloromethane; water; acetone;
DOI:10.1016/j.carres.2015.06.004