2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

Base Information

Chemical Name:2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate
CAS No.:1266621-02-6
Molecular Formula:C₁₆H₁₅N₂OS*ClO₄
Molecular Weight:382.825
Hs Code.:

Synonyms:2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

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Chemical Property of 2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

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Technology Process of 2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

There total 1 articles about 2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 201804-48-0
(E)-1-(4-methoxyphenyl)-3-methylthio-3-(pyridin-2-ylamino)prop-2-en-1-one

: 1266621-02-6
2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

Guidance literature:: With perchloric acid; In methanol; water; at 20 ℃; regioselective reaction;

Reference yield: 55.0%

: 1266621-02-6
2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

: 201804-48-0
(E)-1-(4-methoxyphenyl)-3-methylthio-3-(pyridin-2-ylamino)prop-2-en-1-one

Guidance literature:: With water; sodium hydroxide; In methanol; for 4h;

Reference yield:

: 1266621-02-6
2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium perchlorate

: 2-methylthio-4-(4-methoxyphenyl)pyrido[1,2-a]pyrimidin-5-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / methanol / 4 h

2: boron trifluoride diethyl etherate / benzene / 1 h / Reflux

With boron trifluoride diethyl etherate; water; sodium hydroxide; In methanol; benzene;