(C₆H₅BClAs(C(CH₃)3)2)2

Base Information

Chemical Name:(C₆H₅BClAs(C(CH₃)3)2)2
CAS No.:148098-61-7
Molecular Formula:C₂₈H₄₆As₂B₂Cl₂
Molecular Weight:625.044
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>BClAs(C(CH<sub>3</sub>)3)2)2

Synonyms:(C₆H₅BClAs(C(CH₃)3)2)2

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Chemical Property of (C₆H₅BClAs(C(CH₃)3)2)2

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Technology Process of (C₆H₅BClAs(C(CH₃)3)2)2

There total 1 articles about (C₆H₅BClAs(C(CH₃)3)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 873-51-8
phenylborondichloride

: 819-16-9
di-t-butylarsane

: 148098-61-7
(C₆H₅BClAs(C(CH₃)3)2)2

Guidance literature:: With n-butyl lithium; In diethyl ether; hexane; Schlenk technique or drybox under N2; a stirred soln. of t-Bu2AsH in Et2O is treated dropwise with n-BuLi in hexane with cooling in ice bath, soln. is stirred for 30 min, PhBCl2 in hexane is added, soln. is stirred overnight; volatile compds. are removed under reduced pressure, the residue is taken up in hexane, filtered and concd. and slow cooled in a -20°C freezer;
DOI:10.1021/ja00061a021

Reference yield: 46.0%

: 148098-61-7
(C₆H₅BClAs(C(CH₃)3)2)2

: 19966-87-1
(di-tert-butylarsino)lithium

: 147744-85-2
C₆H₅B(As(C(CH₃)3)2)2

Guidance literature:: In diethyl ether; hexane; Schlenk technique or drybox under N2; a soln. of the boron-compd. in Et2O is treated via cannula with t-Bu2AsLi in hexane, soln. is stirred overnight; solvents are removed under reduced pressure, the residue is extd. with hexane, filtered and concd. and stored overnight in a -20°C freezer, crystn.;
DOI:10.1021/ja00061a021