5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole

Base Information

Chemical Name:5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole
CAS No.:890846-57-8
Molecular Formula:C₁₆H₂₀ClF₂NO₂Si
Molecular Weight:359.876
Hs Code.:

Synonyms:5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole

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Technology Process of 5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole

There total 1 articles about 5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 890133-16-1
2-chloro-3,6-difluoro-benzaldehyde oxime

: 76782-82-6
tert-Butyldimethyl(prop-2-ynyloxy)silane

: 890846-57-8
5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole

Guidance literature:: 2-chloro-3,6-difluoro-benzaldehyde oxime; With pyridine; N-chloro-succinimide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

tert-Butyldimethyl(prop-2-ynyloxy)silane; With triethylamine; In N,N-dimethyl-formamide; at 85 ℃; for 1.58333h;

Reference yield: 98.0%

: 890846-57-8
5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole

: 890846-58-9
[3-(2-chloro-3,6-difluoro-phenyl)-isoxazol-5-yl]-methanol

Guidance literature:: 5-(tert-butyldimethylsilanyloxymethyl)-3-(2-chloro-3,6-difluorophenyl)isoxazole; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; water;