Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester

Base Information

• Chemical Name: Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester
• CAS No.: 96916-44-8
• Molecular Formula: C₁₀H₇Cl₃O₃
• Molecular Weight: 281.523

Synonyms:Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester

Chemical Property of Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester

Chemical Property:

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Technology Process of Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester

There total 1 articles about Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Isopropenyl chloroformate (57933-83-2) + sodium 2,4,6-trichlorophenolate (3784-03-0) → Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester (96916-44-8)

Guidance literature:

In acetonitrile; Ambient temperature;

DOI:10.1016/S0040-4039(00)98321-7

Reference yield: 91.0%

Nα-(tert-butyloxycarbonyl)-L-proline (15761-39-4,59433-50-0) + Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester (96916-44-8) → Pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-(2,4,6-trichloro-phenyl) ester (96916-48-2)

Guidance literature:

With 4-methyl-morpholine; In acetonitrile;

DOI:10.1016/S0040-4039(00)98321-7

Reference yield: 90.0%

N-t-butyloxycarbonyl-L-alanine (3744-87-4,7764-95-6,15761-38-3) + Carbonic acid isopropenyl ester 2,4,6-trichloro-phenyl ester (96916-44-8) → 2-tert-Butoxycarbonylamino-propionic acid 2,4,6-trichloro-phenyl ester (96916-46-0)

Guidance literature:

With 4-methyl-morpholine; In acetonitrile;

DOI:10.1016/S0040-4039(00)98321-7

upstream raw materials:

Isopropenyl chloroformate

sodium 2,4,6-trichlorophenolate

Downstream raw materials:

(tert.-Butoxycarbonyl)glycin-2,4,6-trichlorphenylester

2-tert-Butoxycarbonylamino-3-methyl-butyric acid 2,4,6-trichloro-phenyl ester

2-tert-Butoxycarbonylamino-3-phenyl-propionic acid 2,4,6-trichloro-phenyl ester

2-tert-Butoxycarbonylamino-propionic acid 2,4,6-trichloro-phenyl ester

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