(Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate

Base Information

Chemical Name:(Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate
CAS No.:1233735-64-2
Molecular Formula:C₁₉H₂₀N₂O₃
Molecular Weight:324.379
Hs Code.:

Synonyms:(Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate

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Technology Process of (Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate

There total 1 articles about (Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2-methylprop-2-en-1-yl 1H-imidazole-1-carboxylate

: 1233735-72-2
1-(1-phenyl-1H-imidazol-2-yl)pent-4-en-1-one

: 1233735-64-2
(Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate

Guidance literature:: 1-(1-phenyl-1H-imidazol-2-yl)pent-4-en-1-one; With sodium hexamethyldisilazane; In 1,2-dimethoxyethane; at -78 ℃; for 0.5h; Inert atmosphere;

2-methylprop-2-en-1-yl 1H-imidazole-1-carboxylate; With boron trifluoride diethyl etherate; In 1,2-dimethoxyethane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja103771w

Reference yield: 75.0%

: 1233735-64-2
(Z)-2-methylallyl-1-(1-phenyl-1H-imidazol-2-yl)penta-1,4-dienyl carbonate

: 1233735-82-4
(S)-2-allyl-4-methyl-1-(1-phenyl-1H-imidazol-2-yl)pent-4-en-1-one

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (R,R)-ANDEN-phenyl Trost ligand; In 1,4-dioxane; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja103771w