C₄₄H₂₇N₅O₂

Base Information

• Chemical Name: C₄₄H₂₇N₅O₂
• CAS No.: 1268851-61-1
• Molecular Formula: C₄₄H₂₇N₅O₂
• Molecular Weight: 657.731
• Mol file: 1268851-61-1.mol

Synonyms:C₄₄H₂₇N₅O₂

Chemical Property of C₄₄H₂₇N₅O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₂₇N₅O₂

There total 2 articles about C₄₄H₂₇N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C44H29N5O2 → C44H27N5O2 (1268851-61-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ol1031848

Reference yield:

meso-tetraphenylporphyrin-2,3-dione → C44H27N5O2 (1268851-61-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride / pyridine / 24 h / 20 °C / Inert atmosphere

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

With hydroxylamine hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In pyridine; dichloromethane;

DOI:10.1021/ol1031848

Reference yield: 95.0%

C44H27N5O2 (1268851-61-1) → C44H28N6O

Guidance literature:

With hydroxylamine hydrochloride; In pyridine; for 2h; Inert atmosphere; Reflux;

DOI:10.1021/ol1031848

Downstream raw materials:

C₄₄H₂₆N₆O

C₄₄H₂₆N₆

C₄₄H₂₄N₆Ni