methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

Base Information

Chemical Name:methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate
CAS No.:110512-41-9
Molecular Formula:C₂₃H₃₃N₃O₁₀
Molecular Weight:511.529
Hs Code.:

methyl N-<N-(benzyloxycarbonyl)-L-alanyl-L-alanyl>-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

Synonyms:methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

Chemical Property:

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Technology Process of methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

There total 4 articles about methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 16946-96-6
N-Cbz-L-alanyl-L-alanine succinimido ester

: 106174-54-3
methyl 8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

: 110512-41-9
methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

Guidance literature:: In tetrahydrofuran; methanol; 1.) 0 deg C, 1 h, 2.) RT, 2 h;
DOI:10.1021/jm00395a022

Reference yield:

: 106174-63-4
methyl 2,6-anhydro-3-deoxy-D-glycero-D-talo-octonate

: 110512-41-9
methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / lithium azide, tetrabromomethane, triphenylphosphine / dimethylformamide / Ambient temperature

2: 90 percent / H₂ / Pd/C / methanol; tetrahydrofuran; ethyl acetate / 2250.2 - 3000.2 Torr

3: 75 percent / tetrahydrofuran; methanol / 1.) 0 deg C, 1 h, 2.) RT, 2 h

With lithium azide; carbon tetrabromide; hydrogen; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00395a022

Reference yield:

: 106174-79-2
methyl 2,6-anhydro-8-azido-3,8-dideoxy-D-glycero-D-talo-octonate

: 110512-41-9
methyl N--8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂ / Pd/C / methanol; tetrahydrofuran; ethyl acetate / 2250.2 - 3000.2 Torr

2: 75 percent / tetrahydrofuran; methanol / 1.) 0 deg C, 1 h, 2.) RT, 2 h

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1021/jm00395a022