C₄₇H₆₄N₂O₆

Base Information

Chemical Name:C₄₇H₆₄N₂O₆
CAS No.:1313606-17-5
Molecular Formula:C₄₇H₆₄N₂O₆
Molecular Weight:753.035
Hs Code.:

C<sub>47</sub>H<sub>64</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₄₇H₆₄N₂O₆

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Chemical Property of C₄₇H₆₄N₂O₆

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Technology Process of C₄₇H₆₄N₂O₆

There total 5 articles about C₄₇H₆₄N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1313606-13-1
C₄₉H₆₈N₂O₆

: 1313606-17-5
C₄₇H₆₄N₂O₆

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 50 ℃; for 4h; Inert atmosphere;
DOI:10.1002/chem.201100180

Reference yield:

: C₁₂H₂₀INO

: 1313606-17-5
C₄₇H₆₄N₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine; benzotriazol-1-ol / dichloromethane / 0 °C / Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

3.1: 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 - 20 °C / Inert atmosphere

3.2: 18 h / Inert atmosphere

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 4 h / 50 °C / Inert atmosphere

With 4-methyl-morpholine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; benzotriazol-1-ol; 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In dichloromethane; N,N-dimethyl-formamide; toluene; 2.1: Stille coupling;
DOI:10.1002/chem.201100180

Reference yield:

: 947412-29-5
(2E,4E,6S,7S,8E)-1-(2-trimethylsilylethoxycarbonylamino)-9-iodo-2,5,7-trimethylnona-2,4,8-trien-6-ol

: 1313606-17-5
C₄₇H₆₄N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetraethylammonium fluoride / acetonitrile / 16 h / 40 °C / Inert atmosphere

2.1: 4-methyl-morpholine; benzotriazol-1-ol / dichloromethane / 0 °C / Inert atmosphere

2.2: 16 h / 20 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

4.1: 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 - 20 °C / Inert atmosphere

4.2: 18 h / Inert atmosphere

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 4 h / 50 °C / Inert atmosphere

With 4-methyl-morpholine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; tetraethylammonium fluoride; benzotriazol-1-ol; 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: Stille coupling;
DOI:10.1002/chem.201100180