N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N⁶-benzoyladenosine

Base Information

• Chemical Name: N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N⁶-benzoyladenosine
• CAS No.: 132850-09-0
• Molecular Formula: C₉₅H₉₅Cl₄N₁₅O₁₉P₂Si₂
• Molecular Weight: 2010.82

Synonyms:N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N⁶-benzoyladenosine

Chemical Property of N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N⁶-benzoyladenosine

Chemical Property:

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Technology Process of N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N⁶-benzoyladenosine

There total 1 articles about N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N⁶-benzoyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate) (132849-87-7) + 2',3'-Anhydro-N6-benzoyladenosine (132849-75-3) → N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N6-benzoyladenosine (132850-09-0)

Guidance literature:

With 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride; In pyridine; for 23h; Ambient temperature;

DOI:10.1002/hlca.19910740104

Reference yield:

N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-2',3'-anhydro-N6-benzoyladenosine (132850-09-0) → C62H79N15O16P2Si2

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

DOI:10.1021/jm00106a015

upstream raw materials:

N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate)

2',3'-Anhydro-N⁶-benzoyladenosine

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