4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

Base Information

Chemical Name:4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole
CAS No.:1443334-66-4
Molecular Formula:C₂₉H₃₆ClN₃O₅S
Molecular Weight:574.141
Hs Code.:

Synonyms:4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

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Chemical Property of 4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

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Technology Process of 4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

There total 5 articles about 4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 17702-11-3
3-methoxypropyl isothiocyanate

: 1443333-08-1
1-(6-amino-6-deoxy-β-D-glucopyranosyl)-4-chloro-3-(4-cyclopropylbenzyl)-1H-indole

: 1443334-66-4
4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/j.bmc.2016.03.058

Reference yield:

: N-indolylglucoside 4-chloro-3-(4-cyclopropylbenzyl)-1-(β-D-glucopyranosyl)-1H-indole

: 1443334-66-4
4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 3 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 80 °C

3: acetic acid; zinc / tetrahydrofuran / 20 °C / Inert atmosphere

4: pyridine / 20 °C

With pyridine; sodium azide; acetic acid; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2016.03.058

Reference yield:

: C₂₅H₂₈ClNO₇S

: 1443334-66-4
4-chloro-3-(4-cyclopropylbenzyl)-1-(6-deoxy-6-{[(3-methoxypropyl)carbamothioyl]-amino}-β-D-glucopyranosyl)-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 80 °C

2: acetic acid; zinc / tetrahydrofuran / 20 °C / Inert atmosphere

3: pyridine / 20 °C

With pyridine; sodium azide; acetic acid; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2016.03.058