1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

Base Information

Chemical Name:1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine
CAS No.:117490-49-0
Molecular Formula:C₃₆H₃₈F₁₆N₄O₆
Molecular Weight:926.695
Hs Code.:

Synonyms:1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

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Chemical Property of 1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

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Technology Process of 1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

There total 3 articles about 1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 28493-86-9
4-nitrophenyl 4-{[(benzyloxy)carbonyl]amino}butanoate

: 117490-47-8
1,12-diamino-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecane

: 117490-49-0
1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

Guidance literature:: With triethylamine; In methanol; chloroform; at 60 ℃;
DOI:10.1016/S0022-1139(00)85027-7

Reference yield:

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

: 117490-49-0
1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCCI / CH₂Cl₂ / Ambient temperature

2: 41 percent / NEt₃ / CHCl₃; methanol / 60 °C

With triethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; chloroform;
DOI:10.1016/S0022-1139(00)85027-7

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 117490-49-0
1,12-bis(N-carbobenzoxy-4-aminobutyryl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-hexadecafluorododecanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 4N NaOH / H₂O

2: 80 percent / DCCI / CH₂Cl₂ / Ambient temperature

3: 41 percent / NEt₃ / CHCl₃; methanol / 60 °C

With sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; chloroform; water;
DOI:10.1016/S0022-1139(00)85027-7