3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

Base Information

Chemical Name:3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole
CAS No.:156092-42-1
Molecular Formula:C₃₂H₃₃N₅O₅
Molecular Weight:567.645
Hs Code.:

Synonyms:3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

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Chemical Property of 3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

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Technology Process of 3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

There total 3 articles about 3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 156092-40-9
5-amino-4-(5-methyl-1,2,4-oxadiazol-3-yl)-1-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-1H-pyrazole

: 156092-42-1
3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 100 ℃; for 1.5h;
DOI:10.1080/15257779408013250

Reference yield:

: 156092-39-6
5-amino-1-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazole-4-carboxamidoxime

: 156092-42-1
3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaOEt / ethyl acetate; ethanol / 8 h / Heating

2: 65 percent / NaH / dimethylformamide / 1.5 h / 100 °C

With sodium ethanolate; sodium hydride; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1080/15257779408013250

Reference yield:

: 64295-48-3
5-amino-1-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazole-4-carbonitrile

: 156092-42-1
3-acetamido-6-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)pyrazolo<3,4-c>pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / NH₂OH, Et₃N / ethanol / 5 h / Heating

2: 76 percent / NaOEt / ethyl acetate; ethanol / 8 h / Heating

3: 65 percent / NaH / dimethylformamide / 1.5 h / 100 °C

With hydroxylamine; sodium ethanolate; sodium hydride; triethylamine; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1080/15257779408013250