(4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Base Information

Chemical Name:(4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)
CAS No.:111570-99-1
Molecular Formula:C₂₂H₂₇NO₁₀
Molecular Weight:465.457
Hs Code.:

(4-acetyl-phenyl)-(tri-<i>O</i>-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Synonyms:(4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Suppliers and Price of (4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Chemical Property:

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Technology Process of (4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

There total 4 articles about (4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 99-93-4
4-Hydroxyacetophenone

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 111570-99-1
(4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Guidance literature:: With 15-crown-5; sodium hydrogencarbonate; In acetonitrile; at 20 ℃;
DOI:10.1023/A:1012988719296

Reference yield:

: 10034-19-2,1191127-63-5
1,3,4,6-tetra-O-acetyl-2-amino-2-deoxy-α-D-glucopyranose hydrochloride

: 111570-99-1
(4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: acetic acid anhydride; hydrogen chloride

3: acetone; aq. NaOH solution

With pyridine; hydrogenchloride; sodium hydroxide; acetic anhydride; acetone;
DOI:10.1039/jr9570004754

Reference yield:

: 3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,76375-61-6,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3
2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose

: 111570-99-1
(4-acetyl-phenyl)-(tri-O-acetyl-2-acetylamino-2-deoxy-β-D-glucopyranoside)

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid anhydride; hydrogen chloride

2: acetone; aq. NaOH solution

With hydrogenchloride; sodium hydroxide; acetic anhydride; acetone;
DOI:10.1039/jr9570004754