C₃₄H₃₄N₈O₉S

Base Information

Chemical Name:C₃₄H₃₄N₈O₉S
CAS No.:1391396-80-7
Molecular Formula:C₃₄H₃₄N₈O₉S
Molecular Weight:730.758
Hs Code.:

C<sub>34</sub>H<sub>34</sub>N<sub>8</sub>O<sub>9</sub>S

Synonyms:C₃₄H₃₄N₈O₉S

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Chemical Property of C₃₄H₃₄N₈O₉S

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Technology Process of C₃₄H₃₄N₈O₉S

There total 26 articles about C₃₄H₃₄N₈O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1399362-69-6
C₄₃H₅₀N₈O₁₁S

: 1391396-80-7
C₃₄H₃₄N₈O₉S

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: C₁₆H₂₆N₂O₆

: 1391396-80-7
C₃₄H₃₄N₈O₉S

Guidance literature:: Multi-step reaction with 18 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethanol

3.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

4.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

5.2: 12 h / -20 - 20 °C / Inert atmosphere

6.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

6.2: pH 1 / Acidic conditions

7.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / ethanol

9.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

10.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

11.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -46 °C / Inert atmosphere

11.2: 12 h / -46 - 20 °C / Inert atmosphere

12.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

13.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

14.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

14.2: 3 h / 0 °C / Inert atmosphere

14.3: 3 h / 20 °C / Inert atmosphere

15.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

15.2: pH 1 / Acidic conditions

16.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

17.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

17.2: pH 1 / Acidic conditions

18.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 14.1: Hantzsch thiazole synthesis / 14.2: Hantzsch thiazole synthesis / 14.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1064764-00-6
methyl 2-(2-methyl-2-tert-butoxy-1-tert-butoxycarbonylamino-ethyl)-oxazole-4-carboxylate

: 1391396-80-7
C₃₄H₃₄N₈O₉S

Guidance literature:: Multi-step reaction with 19 steps

1.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

1.2: pH 1 / Acidic conditions

2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethanol

4.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

6.2: 12 h / -20 - 20 °C / Inert atmosphere

7.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

7.2: pH 1 / Acidic conditions

8.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

9.1: palladium 10% on activated carbon; hydrogen / ethanol

10.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

11.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

12.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -46 °C / Inert atmosphere

12.2: 12 h / -46 - 20 °C / Inert atmosphere

13.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

14.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

15.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

15.2: 3 h / 0 °C / Inert atmosphere

15.3: 3 h / 20 °C / Inert atmosphere

16.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

16.2: pH 1 / Acidic conditions

17.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

18.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

18.2: pH 1 / Acidic conditions

19.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 15.1: Hantzsch thiazole synthesis / 15.2: Hantzsch thiazole synthesis / 15.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105