Technology Process of C33H52N8O12
There total 4 articles about C33H52N8O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
water; acetonitrile;
Inert atmosphere;
Reflux;
DOI:10.1039/c0ob00948b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / methanol / Inert atmosphere; Reflux
2: N-ethyl-N,N-diisopropylamine / water; acetonitrile / Inert atmosphere; Reflux
With
hydrazine hydrate; N-ethyl-N,N-diisopropylamine;
In
methanol; water; acetonitrile;
DOI:10.1039/c0ob00948b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere
2: hydrazine hydrate / methanol / Inert atmosphere; Reflux
3: N-ethyl-N,N-diisopropylamine / water; acetonitrile / Inert atmosphere; Reflux
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c0ob00948b