dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

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Chemical Name:dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate
CAS No.:98331-58-9
Molecular Formula:C₂₃H₁₅NO₈S*2Na
Molecular Weight:511.42
Hs Code.:

Synonyms:dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

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Chemical Property of dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

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Technology Process of dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

There total 10 articles about dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7298-72-8
4-Acetamido-2-allyloxyacetophenone

: 98331-58-9
dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / various solvent(s) / 4 h / Heating

2: 98 percent / H₂ / PtO₂ / acetic acid / 2206.5 Torr

3: 1.) EtONa, 2.) conc. HCl / 1.) ethanol, reflux, 2 h, 2.) ethanol, reflux, 15 h

4: 57 percent / ethanol / 17 h / Heating

5: 81 percent / diphenyl ether / 0.08 h / Heating

6: 59 percent / POCl₃ / benzene / 25 h / Ambient temperature

7: 1,2-dichloro-ethane / 24 h / Heating

8: m-chloroperbenzoic acid / CH₂Cl₂ / 24 h / Ambient temperature

9: 0.1 M NaOH / methanol / 0.25 h / Heating

With hydrogenchloride; sodium hydroxide; hydrogen; sodium ethanolate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; platinum(IV) oxide; In methanol; diphenylether; ethanol; dichloromethane; acetic acid; 1,2-dichloro-ethane; benzene;
DOI:10.1021/jm00150a014

Reference yield:

: 40547-58-8
N-(4-acetyl-3-hydroxyphenyl)acetamide

: 98331-58-9
dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

Guidance literature:: Multi-step reaction with 10 steps

1: 81 percent / potassium carbonate / dimethylformamide / 5 h

2: 70 percent / various solvent(s) / 4 h / Heating

3: 98 percent / H₂ / PtO₂ / acetic acid / 2206.5 Torr

4: 1.) EtONa, 2.) conc. HCl / 1.) ethanol, reflux, 2 h, 2.) ethanol, reflux, 15 h

5: 57 percent / ethanol / 17 h / Heating

6: 81 percent / diphenyl ether / 0.08 h / Heating

7: 59 percent / POCl₃ / benzene / 25 h / Ambient temperature

8: 1,2-dichloro-ethane / 24 h / Heating

9: m-chloroperbenzoic acid / CH₂Cl₂ / 24 h / Ambient temperature

10: 0.1 M NaOH / methanol / 0.25 h / Heating

With hydrogenchloride; sodium hydroxide; hydrogen; sodium ethanolate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; platinum(IV) oxide; In methanol; diphenylether; ethanol; dichloromethane; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00150a014

Reference yield:

: 69069-03-0
1-(4-Acetylamino-3-(prop-2-enyl)-2-hydroxyphenyl)ethanone

: 98331-58-9
dissodium 4-oxo-6-(phenylsulfonyl)-10-propyl-4H-pyrano<3,2-g>quinoline-2,8-dicarboxylate

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / H₂ / PtO₂ / acetic acid / 2206.5 Torr

2: 1.) EtONa, 2.) conc. HCl / 1.) ethanol, reflux, 2 h, 2.) ethanol, reflux, 15 h

3: 57 percent / ethanol / 17 h / Heating

4: 81 percent / diphenyl ether / 0.08 h / Heating

5: 59 percent / POCl₃ / benzene / 25 h / Ambient temperature

6: 1,2-dichloro-ethane / 24 h / Heating

7: m-chloroperbenzoic acid / CH₂Cl₂ / 24 h / Ambient temperature

8: 0.1 M NaOH / methanol / 0.25 h / Heating

With hydrogenchloride; sodium hydroxide; hydrogen; sodium ethanolate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; platinum(IV) oxide; In methanol; diphenylether; ethanol; dichloromethane; acetic acid; 1,2-dichloro-ethane; benzene;
DOI:10.1021/jm00150a014