2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

Base Information

Chemical Name:2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine
CAS No.:101219-02-7
Molecular Formula:C₁₈H₁₄F₅P
Molecular Weight:356.275
Hs Code.:

Synonyms:2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

Chemical Property:

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Technology Process of 2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

There total 1 articles about 2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2548-47-2
2,3-diphenyl-1,3-butadiene

: 39185-13-2
trimethylstannyl-bis(trifluormethyl)phosphane

: 101219-02-7
2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

Guidance literature:: In chloroform; at 70 ℃; for 72h;
DOI:10.1016/S0040-4039(00)89222-9

Reference yield: 52.0%

: 36477-75-5
tungsten pentacarbonyl tetrahydrofuran

: 101219-02-7
2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

: 121334-37-0
W(CO)5C₁₈H₁₄F₅P

Guidance literature:: In not given; Equimolar amounts, 48 h, inert atmosphere.; Distn., 40-50°C/10^-2 torr, elem. anal.;
DOI:10.1016/0022-328X(88)80137-2

Reference yield: 48.0%

: 15038-41-2
pentacarbonyl(tetrahydrofuran)chromium⁽⁰⁾

: 101219-02-7
2,2-Difluoro-4,5-diphenyl-1-trifluoromethyl-1,2,3,6-tetrahydro-phosphinine

: 121334-36-9
Cr(CO)5CF₃PCF₂CH₂C(C₆H₅)C(C₆H₅)CH₂

Guidance literature:: In not given; Equimolar amounts, 24 h, inert atmosphere.; Distn., 30-35°C/10^-2 torr, elem. anal.;
DOI:10.1016/0022-328X(88)80137-2