2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

Base Information

Chemical Name:2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose
CAS No.:88087-34-7
Molecular Formula:C₄₅H₄₉NO₁₁
Molecular Weight:779.884
Hs Code.:

Synonyms:2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

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Chemical Property of 2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

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Technology Process of 2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

There total 4 articles about 2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.7%

: 88087-32-5
3-O-allyl-2-di-O-benzoyl-4,6-di-O-benzyl-α-D-glucopyranosyl bromide

: 50604-73-4
2-Acetamido-1,6-anhydro-3-O-benzyl-2-desoxy-β-D-glucopyranose

: 3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-D-glucopyranose

: 88087-34-7
2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

Guidance literature:: With calcium sulfate; mercury(II) cyanide; In nitromethane; benzene; for 25h; Ambient temperature;

Reference yield:

: 88087-31-4
3-O-allyl-1,2-di-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranose

: 88087-34-7
2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 90.1 percent / 30percent HBr-AcOH / CH₂Cl₂ / 0.67 h / 0 °C

2: 63.7 percent / Hg(CN)2, drierite / benzene; nitromethane / 25 h / Ambient temperature

With calcium sulfate; hydrogen bromide; mercury(II) cyanide; acetic acid; In nitromethane; dichloromethane; benzene;

Reference yield:

: 91595-25-4,91595-46-9
3-O-allyl-4,6-di-O-benzyl-D-glucopyranose

: 88087-34-7
2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-4-O-(3-O-allyl-2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 77.6 percent / pyridine / 18 h / Ambient temperature

2: 90.1 percent / 30percent HBr-AcOH / CH₂Cl₂ / 0.67 h / 0 °C

3: 63.7 percent / Hg(CN)2, drierite / benzene; nitromethane / 25 h / Ambient temperature

With pyridine; calcium sulfate; hydrogen bromide; mercury(II) cyanide; acetic acid; In nitromethane; dichloromethane; benzene;