L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

Base Information

Chemical Name:L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol
CAS No.:200273-12-7
Molecular Formula:C₄₁H₃₄O₉S
Molecular Weight:702.782
Hs Code.:

Synonyms:L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

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Chemical Property of L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

Chemical Property:

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Technology Process of L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

There total 14 articles about L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1005-56-7
phenylcarbonochloridothioate

: 200273-11-6
L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-chiro-inositol

: 200273-12-7
L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

Guidance literature:: With pyridine; dmap; In acetonitrile; for 3h;
DOI:10.1016/S0040-4020(97)10101-6

Reference yield:

: 156593-39-4
methyl 3,4-O-cyclohexylidene-β-D-galactopyranoside

: 200273-12-7
L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

Guidance literature:: Multi-step reaction with 9 steps

1: 90 percent / triphenylphosphine, carbon tetrachloride, pyridine / 8 h / 60 °C

2: 1.) potassium hydroxide, benzyltrimethylammonium chloride / 1.) CH₂Cl₂, 10 min, 2.) CH₂Cl₂, 12 h

3: 30 percent / sodium hydride / dimethylformamide / 3 h / 110 °C

4: 1.) mercury(II) chloride, 2.) thiourea / multistep reaction; 1.) acetone, H₂O, 25 deg C; other reagents: various Hg(II) salts, Hg(NO₃)2/HNO₃, HgCl₂/H₂SO₄, PdCl₂, other temperatures and reaction time, various reactants ratio, 2.) acetone, H₂O, 25 deg C, 2 h, other temperatures

5: 29 percent / cerium(III) chloride heptahydrate, sodium borohydride / methanol / Ambient temperature

6: 90 percent / CH₂Cl₂ / 12 h / 60 °C

7: 89 percent / acetic acid / H₂O / 2 h / 60 °C

8: 78 percent / CH₂Cl₂ / 12 h / 60 °C

9: 84 percent / 4-(dimethylamino)pyridine, pyridine / acetonitrile / 3 h

With pyridine; tetrachloromethane; dmap; potassium hydroxide; sodium tetrahydroborate; cerium(III) chloride; benzyltrimethylammonium chloride; sodium hydride; acetic acid; thiourea; triphenylphosphine; mercury dichloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(97)10101-6

Reference yield:

: 1824-94-8
methyl beta-D-galactopyranoside

: 200273-12-7
L-2,4,5-tri-O-benzoyl-1-O-benzyl-3-deoxy-6-O-phenoxythiocarbonyl-chiro-inositol

Guidance literature:: Multi-step reaction with 10 steps

1: 90 percent / H₂SO₄ / dimethylformamide / 12 h / Ambient temperature

2: 90 percent / triphenylphosphine, carbon tetrachloride, pyridine / 8 h / 60 °C

3: 1.) potassium hydroxide, benzyltrimethylammonium chloride / 1.) CH₂Cl₂, 10 min, 2.) CH₂Cl₂, 12 h

4: 30 percent / sodium hydride / dimethylformamide / 3 h / 110 °C

5: 1.) mercury(II) chloride, 2.) thiourea / multistep reaction; 1.) acetone, H₂O, 25 deg C; other reagents: various Hg(II) salts, Hg(NO₃)2/HNO₃, HgCl₂/H₂SO₄, PdCl₂, other temperatures and reaction time, various reactants ratio, 2.) acetone, H₂O, 25 deg C, 2 h, other temperatures

6: 29 percent / cerium(III) chloride heptahydrate, sodium borohydride / methanol / Ambient temperature

7: 90 percent / CH₂Cl₂ / 12 h / 60 °C

8: 89 percent / acetic acid / H₂O / 2 h / 60 °C

9: 78 percent / CH₂Cl₂ / 12 h / 60 °C

10: 84 percent / 4-(dimethylamino)pyridine, pyridine / acetonitrile / 3 h

With pyridine; tetrachloromethane; dmap; potassium hydroxide; sodium tetrahydroborate; cerium(III) chloride; sulfuric acid; benzyltrimethylammonium chloride; sodium hydride; acetic acid; thiourea; triphenylphosphine; mercury dichloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(97)10101-6