3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

Base Information

Chemical Name:3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione
CAS No.:1620951-88-3
Molecular Formula:C₂₇H₂₄N₄O₄
Molecular Weight:468.512
Hs Code.:

Synonyms:3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

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Chemical Property of 3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

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Technology Process of 3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

There total 10 articles about 3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.83%

: 1620951-87-2
3-(2-(4'-(4-((tetrahydro-2H-pyran-2-yl)oxy)butoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

: 1620951-88-3
3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; at 0 ℃; for 0.5h;

Reference yield:

: 1620955-35-2
C₃₁H₃₄N₄O₄

: 1620951-88-3
3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 3.45 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane; methanol / 0.5 h / 0 °C

With hydrogenchloride; In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 1620955-33-0
C₂₉H₃₁N₃O₃

: 1620951-88-3
3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 0 - 20 °C / Inert atmosphere

2: piperidine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

3: dichloromethane / 3.45 h / 0 - 20 °C / Inert atmosphere

4: hydrogenchloride / 1,4-dioxane; methanol / 0.5 h / 0 °C

With piperidine; hydrogenchloride; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;