1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate
CAS No.:1004755-34-3
Molecular Formula:C₃₀H₃₂Cl₂N₂O₄
Molecular Weight:555.501
Hs Code.:

Synonyms:1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

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Chemical Property of 1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

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Technology Process of 1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

There total 1 articles about 1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1004755-00-3,1149765-08-1
1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

: 122-78-1
phenylacetaldehyde

: 1004755-34-3
1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

: 1004755-35-4
1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1S)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

Guidance literature:: 1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate; With n-butyllithium; diisopropylamine; 1,10-Phenanthroline; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.916667h;

phenylacetaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 3.25h; Product distribution / selectivity;

Reference yield: 94.0%

: 1004755-34-3
1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate

: 1004755-36-5
(3R)-hydroxy-4-phenyl-(2S)-[(1'R)-(phenylethyl)amino]butanoic acid

: (3S)-hydroxy-4-phenyl-(2S)-[(1'R)-(phenylethyl)amino]butanoic acid

Guidance literature:: 1,1-dimethylethyl (2R)-(2,6-dichlorophenyl)-4-((1R)-hydroxy-2-phenylethyl)-5-oxo-3-((1'R)-phenylethyl)tetrahydro-1H-1-imidazolecarboxylate; With hydrogenchloride; water; at 120 - 130 ℃; for 4.5h;

With sodium hydroxide; water; at 0 ℃; for 2h; pH=6 - 7;