Technology Process of C15H18Br2O2
There total 4 articles about C15H18Br2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H20Br2O2;
With
boron trichloride; tetra-(n-butyl)ammonium iodide;
In
dichloromethane;
at -78 - -10 ℃;
Inert atmosphere;
With
water; sodium hydrogencarbonate;
In
dichloromethane;
chemoselective reaction;
Inert atmosphere;
DOI:10.1039/c0cc01419b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
2.1: boron trichloride; tetra-(n-butyl)ammonium iodide / dichloromethane / -78 - -10 °C / Inert atmosphere
2.2: Inert atmosphere
With
carbon tetrabromide; boron trichloride; tetra-(n-butyl)ammonium iodide; triphenylphosphine;
In
dichloromethane;
DOI:10.1039/c0cc01419b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 2.17 h / 20 °C / Inert atmosphere
2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
3.1: boron trichloride; tetra-(n-butyl)ammonium iodide / dichloromethane / -78 - -10 °C / Inert atmosphere
3.2: Inert atmosphere
With
lithium aluminium tetrahydride; carbon tetrabromide; boron trichloride; tetra-(n-butyl)ammonium iodide; triphenylphosphine;
In
diethyl ether; dichloromethane;
DOI:10.1039/c0cc01419b