(2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate

Base Information

Chemical Name:(2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate
CAS No.:1009316-51-1
Molecular Formula:C₄₃H₆₃N₃O₆SSi
Molecular Weight:778.141
Hs Code.:

Synonyms:(2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate

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Technology Process of (2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate

There total 1 articles about (2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-3-hydroxyoctadecan-4-yl 4-methylbenzenesulfonate

: 108-24-7
acetic anhydride

: 1009316-51-1
(2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1021/jo702147y

Reference yield:

: 1009316-51-1
(2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate

: (2S,3S,4S)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-3,4-diol

Guidance literature:: (2S,3S,4R)-2-azido-1-(tert-butyl(diphenyl)silyloxy)-4-(tosyloxy)octadecan-3-yl acetate; With calcium carbonate; In ethanol; water; for 4h; Heating;

With potassium carbonate; In methanol; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo702147y