2-Bromo-4-methylbenzamide

Base Information

Chemical Name:2-Bromo-4-methylbenzamide
CAS No.:131002-03-4
Molecular Formula:C₈H₈BrNO
Molecular Weight:214.062
Hs Code.:
NSC Number:95797
DSSTox Substance ID:DTXSID201312307
Nikkaji Number:J340.483H

Synonyms:2-bromo-4-methylbenzamide;131002-03-4;NSC95797;2-Bromo-4-methyl-benzamide;SCHEMBL305165;DTXSID201312307;MFCD18392004;NSC-95797;AKOS017552495;CS-0191567;E91505

Suppliers and Price of 2-Bromo-4-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Bromo-4-methylbenzamide

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:212.97893
Heavy Atom Count:11
Complexity:160

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)C(=O)N)Br

Technology Process of 2-Bromo-4-methylbenzamide

There total 8 articles about 2-Bromo-4-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7697-27-0
2-bromo-4-methylbenzoic acid

: 131002-03-4
4-methyl-2- bromobenzamide

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 50 ℃; for 3h;

Reference yield: 70.0%

: 619-55-6
para-methylbenzamide

: 131002-03-4
4-methyl-2- bromobenzamide

: 2,6-dibromo-4-methyl-benzoic acid amide

Guidance literature:: With N-Bromosuccinimide; palladium diacetate; trifluoroacetic acid; In 1,2-dichloro-ethane; at 60 ℃; for 24h; regioselective reaction; Sealed tube;
DOI:10.1016/j.catcom.2019.105784

Reference yield: 68.0%

: 619-55-6
para-methylbenzamide

: 131002-03-4
4-methyl-2- bromobenzamide

Guidance literature:: With N-Bromosuccinimide; silver hexafluoroantimonate; trifluorormethanesulfonic acid; nickel diacetate; In 1,2-dichloro-ethane; at 80 ℃; for 12h; regioselective reaction;
DOI:10.1039/C8NJ06023A