8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

Base Information

Chemical Name:8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline
CAS No.:112378-05-9
Molecular Formula:C₃₃H₂₈BrNO₆
Molecular Weight:614.492
Hs Code.:

Synonyms:8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

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Chemical Property of 8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

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Technology Process of 8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

There total 1 articles about 8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 36547-83-8
2-benzoyl-8-benzyloxy-1,2-dihydro-7-methoxy-isoquinoline-1-carbonitrile

: 112378-05-9
8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In benzene; for 5h;

Reference yield:

: 112378-05-9
8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

: 112378-08-2
1-(2'-bromo-4',5'-dimethoxybenzoyl)-7-methoxyisoquinolin-8-ol

Guidance literature:: Multi-step reaction with 3 steps

1: OH^-

2: 88 percent / pyridinium dichromate / CH₂Cl₂ / 48 h

3: H⁺

With dipyridinium dichromate; hydroxide; hydrogen cation; In dichloromethane;

Reference yield:

: 112378-05-9
8-benzyloxy-1-(2'-bromo-α-benzoyloxy-4',5'-dimethoxybenzyl)-7-methoxyisoquinoline

: 112378-07-1
8-benzyloxy-1-(2'-bromo-4',5'-dimethoxybenzoyl)-7-methoxyisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: OH^-

2: 88 percent / pyridinium dichromate / CH₂Cl₂ / 48 h

With dipyridinium dichromate; hydroxide; In dichloromethane;