(E)-3-methyl-5-phenyl-2-penteneamide

Base Information

Chemical Name:(E)-3-methyl-5-phenyl-2-penteneamide
CAS No.:72681-06-2
Molecular Formula:C₁₂H₁₅NO
Molecular Weight:189.257
Hs Code.:

Synonyms:(E)-3-methyl-5-phenyl-2-penteneamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-methyl-5-phenyl-2-penteneamide

Chemical Property:

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Technology Process of (E)-3-methyl-5-phenyl-2-penteneamide

There total 5 articles about (E)-3-methyl-5-phenyl-2-penteneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-3-methyl-5-phenyl-2-pentenoyl chloride

: 72681-06-2
(E)-3-methyl-5-phenyl-2-penteneamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jacs.5b06418

Reference yield:

: 72681-05-1
(E/Z)-3-methyl-5-phenylpent-2-enoic acid

: 72681-06-2
(E)-3-methyl-5-phenyl-2-penteneamide

Guidance literature:: Multistep reaction; (i) PCl₃, (ii) NH₃;
DOI:10.1002/hlca.19790620733

Reference yield:

: 2550-26-7
4-Phenyl-2-butanone

: 72681-06-2
(E)-3-methyl-5-phenyl-2-penteneamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / -70 °C

2: (COCl)2 / CH₂Cl₂

3: aq. NH₃ / tetrahydrofuran

With ammonium hydroxide; oxalyl dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(00)86123-6