dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Base Information

Chemical Name:dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate
CAS No.:1329454-67-2
Molecular Formula:C₃₃H₄₈O₁₄
Molecular Weight:668.736
Hs Code.:

Synonyms:dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

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Chemical Property of dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

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Technology Process of dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

There total 2 articles about dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1166-52-5
dodecyl gallate

: 1329454-67-2
dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: camphor-10-sulfonic acid / chloroform / 16 h / 60 °C

2: boron trifluoride diethyl etherate / dichloromethane

3: trifluoroacetic acid / 24 h / 20 °C

With camphor-10-sulfonic acid; boron trifluoride diethyl etherate; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1016/j.tet.2011.07.046

Reference yield:

: 1329454-39-8
C₂₂H₃₄O₅

: 1329454-67-2
dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: trifluoroacetic acid / 24 h / 20 °C

With boron trifluoride diethyl etherate; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.tet.2011.07.046

Reference yield: 100.0%

: 1329454-67-2
dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

: 1329454-80-9
dodecyl 3-O-(β-D-glucopyranosyl)-4,5-dihydroxybenzoate

Guidance literature:: dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate; With methanol; sodium carbonate; for 1h;

IR-120; In methanol; pH=7;
DOI:10.1016/j.tet.2011.07.046