Technology Process of dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate
There total 2 articles about dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: camphor-10-sulfonic acid / chloroform / 16 h / 60 °C
2: boron trifluoride diethyl etherate / dichloromethane
3: trifluoroacetic acid / 24 h / 20 °C
With
camphor-10-sulfonic acid; boron trifluoride diethyl etherate; trifluoroacetic acid;
In
dichloromethane; chloroform;
DOI:10.1016/j.tet.2011.07.046
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / dichloromethane
2: trifluoroacetic acid / 24 h / 20 °C
With
boron trifluoride diethyl etherate; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.tet.2011.07.046
- Guidance literature:
-
dodecyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate;
With
methanol; sodium carbonate;
for 1h;
IR-120;
In
methanol;
pH=7;
DOI:10.1016/j.tet.2011.07.046
