N-(5-methyl-2-nitrophenyl)-4-benzamide

Base Information

Chemical Name:N-(5-methyl-2-nitrophenyl)-4-benzamide
CAS No.:1025886-13-8
Molecular Formula:C₂₂H₂₀N₄O₅
Molecular Weight:420.425
Hs Code.:

N-(5-methyl-2-nitrophenyl)-4-<N-(pyridin-3-ylmethylcarbonyl)aminomethyl>benzamide

Synonyms:N-(5-methyl-2-nitrophenyl)-4-benzamide

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Chemical Property of N-(5-methyl-2-nitrophenyl)-4-benzamide

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Technology Process of N-(5-methyl-2-nitrophenyl)-4-benzamide

There total 4 articles about N-(5-methyl-2-nitrophenyl)-4-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 578-46-1
5-methyl-2-nitroaniline

: 4-benzoyl chloridehydrochloride

: 1025886-13-8
N-(5-methyl-2-nitrophenyl)-4-benzamide

Guidance literature:: With pyridine; for 1h;
DOI:10.1021/jm980565u

Reference yield:

: 100-55-0
3-hydroxymethylpyridin

: 1025886-13-8
N-(5-methyl-2-nitrophenyl)-4-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 1 h / Ambient temperature

2: DBU, Et₃N / tetrahydrofuran / 5 h / Ambient temperature

3: (COCl)2, DMF / toluene / 4 h

4: 54 percent / pyridine / 1 h

With pyridine; oxalyl dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; toluene;
DOI:10.1021/jm980565u

Reference yield:

: 212632-27-4
pyridin-3-ylmethyl 1H-imidazole-1-carboxylate

: 1025886-13-8
N-(5-methyl-2-nitrophenyl)-4-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: DBU, Et₃N / tetrahydrofuran / 5 h / Ambient temperature

2: (COCl)2, DMF / toluene / 4 h

3: 54 percent / pyridine / 1 h

With pyridine; oxalyl dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; toluene;
DOI:10.1021/jm980565u