N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

Base Information

Chemical Name:N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine
CAS No.:886055-96-5
Molecular Formula:C₂₁H₃₁FN₂O₄
Molecular Weight:394.487
Hs Code.:

Synonyms:N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

Chemical Property:

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Technology Process of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

There total 3 articles about N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 843651-78-5
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]hydrazine

: 886055-96-5
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

Guidance literature:: N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]hydrazine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

ethyl halide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm050538l

Reference yield:

: 350-40-3
2-(4-fluorophenyl)-1-propene

: 886055-96-5
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: NBS / CCl₄ / Heating

2.1: NaH / dimethylformamide / 0.33 h / 20 °C

2.2: 89 percent / dimethylformamide / 7 h / 20 °C

3.1: NaH / dimethylformamide / 0.33 h / 20 °C

3.2: 93 percent / dimethylformamide / 20 °C

With N-Bromosuccinimide; sodium hydride; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050538l

Reference yield:

: 132927-05-0
1-(3-bromoprop-1-en-2-yl)-4-fluorobenzene

: 886055-96-5
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-ethylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.33 h / 20 °C

1.2: 89 percent / dimethylformamide / 7 h / 20 °C

2.1: NaH / dimethylformamide / 0.33 h / 20 °C

2.2: 93 percent / dimethylformamide / 20 °C

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm050538l