(2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol

Base Information

Chemical Name:(2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol
CAS No.:1000153-24-1
Molecular Formula:C₂₇H₃₆O₅
Molecular Weight:440.58
Hs Code.:

Synonyms:(2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol

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Chemical Property of (2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol

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Technology Process of (2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol

There total 2 articles about (2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: (PMBOCH₂CH₂C)2

: 22742-89-8
2-methyl-2,3-butadiene-1-ol

: 1000153-24-1
(2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol

Guidance literature:: (PMBOCH₂CH₂C)2; With triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride; In diethyl ether; hexane; toluene; at -78 - -30 ℃;

2-methyl-2,3-butadiene-1-ol; With n-butyllithium; In diethyl ether; hexane; toluene; at -78 - 0 ℃; Further stages.;
DOI:10.1039/b708256h

Reference yield: 74.0%

: (PMBOCH₂CH₂C)2

: C₅H₇O^(1-)*Li⁽¹⁺⁾

: 1000153-24-1
(2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methylocta-2,5-dien-1-ol

Guidance literature:: (PMBOCH₂CH₂C)2; With triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride; In diethyl ether; hexane; toluene; at -78 - -30 ℃; for 2h;

C₅H₇O^(1-)*Li⁽¹⁺⁾; In diethyl ether; hexane; toluene; at -78 - 0 ℃; for 2h;

With water; ammonium chloride; In diethyl ether; hexane; toluene; at 0 - 20 ℃; Further stages.;
DOI:10.1016/j.tet.2008.02.015