(S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

Base Information

Chemical Name:(S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate
CAS No.:883149-27-7
Molecular Formula:C₂₁H₁₈N₄O₈S
Molecular Weight:486.462
Hs Code.:

Synonyms:(S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

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Chemical Property of (S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

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Technology Process of (S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

There total 3 articles about (S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 930785-60-7
(S)-methyl 2-(2,4-dinitrobenzenesulfonyl)-3-(1H-indol-3-yl)propanoate

: 106-96-7
propargyl bromide

: 883149-27-7
(S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1002/chem.200601324

Reference yield:

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 883149-27-7
(S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / triethylamine / CH₂Cl₂ / 16 h / 20 °C

2: 45 percent / sodium hydride / dimethylformamide; various solvent(s) / 16 h / 20 °C

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601324

Reference yield:

: 7524-52-9,26988-71-6,5619-09-0,14907-27-8,41222-70-2,67557-19-1,109492-62-8
(S)-tryptophan methyl ester hydrochloride

: 883149-27-7
(S)-methyl 2-(N-(prop-2-ynyl)-N-(2,4-dinitrobenzenesulfonylamino))-3-(1H-indol-3-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / triethylamine / CH₂Cl₂ / 16 h / 20 °C

2: 45 percent / sodium hydride / dimethylformamide; various solvent(s) / 16 h / 20 °C

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601324