Technology Process of C30H30N2O9S
There total 4 articles about C30H30N2O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid / water / 2 h / 20 °C
2.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C
2.2: 2 h / Reflux
3.1: potassium carbonate / methanol / 16 h / 20 °C
With
N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; potassium carbonate;
In
methanol; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C
2.1: sulfuric acid / water / 2 h / 20 °C
3.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C
3.2: 2 h / Reflux
4.1: potassium carbonate / methanol / 16 h / 20 °C
With
dmap; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; potassium carbonate; triethylamine;
In
methanol; dichloromethane; water; acetonitrile;