C₃₄H₇₀O₃Si₂

Base Information

Chemical Name:C₃₄H₇₀O₃Si₂
CAS No.:947321-18-8
Molecular Formula:C₃₄H₇₀O₃Si₂
Molecular Weight:583.099
Hs Code.:

C<sub>34</sub>H<sub>70</sub>O<sub>3</sub>Si<sub>2</sub>

Synonyms:C₃₄H₇₀O₃Si₂

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Chemical Property of C₃₄H₇₀O₃Si₂

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Technology Process of C₃₄H₇₀O₃Si₂

There total 1 articles about C₃₄H₇₀O₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 947321-15-5
C₂₅H₅₀O₃Si

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 947321-18-8
C₃₄H₇₀O₃Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 0.75h;
DOI:10.1021/jo070901r

Reference yield:

: 947321-18-8
C₃₄H₇₀O₃Si₂

: C₅₀H₈₃BrO₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / p-toluenesulfonic acid; ethanol / 0 - 23 °C

2: 91 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 2 h

3: 44 percent / titanium tetrabromide; titanium tetraisopropoxide; 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 2 h / -78 °C

With pyridine; titanium(IV) isopropylate; 2,6-di-tert-butyl-4-methylpyridine; ethanol; titanium(IV) bromide; Dess-Martin periodane; toluene-4-sulfonic acid; In dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1021/jo070901r

Reference yield:

: 947321-18-8
C₃₄H₇₀O₃Si₂

: 947321-28-0
C₃₃H₄₈O₇Se

Guidance literature:: Multi-step reaction with 10 steps

1: 73 percent / p-toluenesulfonic acid; ethanol / 0 - 23 °C

2: 91 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 2 h

3: 53 percent / titanium tetrabromide; titanium tetraisopropoxide; 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 2 h / -78 °C

4: 89 percent / 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 20 h

5: 73 percent / potassium hydroxide; water / acetonitrile; various solvent(s) / 14 h

6: 73 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 0.75 h

7: 89 percent / 2-methyl-2-butene; sodium chlorite; monobasic sodium phosphate / 2-methyl-propan-2-ol; H₂O / 2 h

8: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0 - 23 °C

9: 75 percent / tributylphosphine; diisopropyl azodicarboxylate / toluene / 0.83 h

10: 78 percent / 18-crown-6 / toluene / 16 h / 110 °C

With pyridine; titanium(IV) isopropylate; potassium hydroxide; sodium chlorite; 2,6-di-tert-butyl-4-methylpyridine; 2-methyl-but-2-ene; 18-crown-6 ether; ethanol; tributylphosphine; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; water; titanium(IV) bromide; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 2: Dess-Martin oxidation / 6: Dess-Martin oxidation / 7: Lindgren oxidation / 9: Mitsunobu reaction;
DOI:10.1021/jo070901r