C₁₅H₁₄N₂O

Base Information

Chemical Name:C₁₅H₁₄N₂O
CAS No.:1353687-01-0
Molecular Formula:C₁₅H₁₄N₂O
Molecular Weight:238.289
Hs Code.:

C<sub>15</sub>H<sub>14</sub>N<sub>2</sub>O

Synonyms:C₁₅H₁₄N₂O

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Chemical Property of C₁₅H₁₄N₂O

Chemical Property:

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Technology Process of C₁₅H₁₄N₂O

There total 7 articles about C₁₅H₁₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₁₅H₁₅ClN₂O

: 1353687-01-0
C₁₅H₁₄N₂O

Guidance literature:: With potassium; tert-butyl alcohol; In N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c1ob06423a

Reference yield:

: 81417-99-4
1-(pyridin-2-yl)pent-4-en-1-ol

: 1353687-01-0
C₁₅H₁₄N₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 °C / Inert atmosphere

2.1: n-butyllithium / hexanes; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2.2: 18 h / 0 - 20 °C / Inert atmosphere

2.3: 20 °C / Inert atmosphere

3.1: methanol; potassium carbonate / 2 h / 20 °C

4.1: ethanol / 4 h / 100 °C / Inert atmosphere

5.1: benzene / 24 h / 80 °C / Inert atmosphere

6.1: potassium; tert-butyl alcohol / N,N,N,N,N,N-hexamethylphosphoric triamide / 0.5 h / -78 - 20 °C / Inert atmosphere

With methanol; n-butyllithium; oxalyl dichloride; potassium; potassium carbonate; dimethyl sulfoxide; tert-butyl alcohol; In N,N,N,N,N,N-hexamethylphosphoric triamide; hexanes; diethyl ether; ethanol; dichloromethane; benzene; 1.1: Swern oxidation / 5.1: Diels-Alder reaction;
DOI:10.1039/c1ob06423a

Reference yield:

: 1353686-79-9
C₁₂H₁₃NO

: 1353687-01-0
C₁₅H₁₄N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 24 h / 80 °C / Inert atmosphere

2: potassium; tert-butyl alcohol / N,N,N,N,N,N-hexamethylphosphoric triamide / 0.5 h / -78 - 20 °C / Inert atmosphere

With potassium; tert-butyl alcohol; In N,N,N,N,N,N-hexamethylphosphoric triamide; benzene; 1: Diels-Alder reaction;
DOI:10.1039/c1ob06423a