4cis.6cis.8cis.2trans-1.2.4.7-Tetraphenyl-cyclooctatetraen

Base Information

• Chemical Name: 4cis.6cis.8cis.2trans-1.2.4.7-Tetraphenyl-cyclooctatetraen
• CAS No.: 19099-38-8
• Molecular Formula: C₃₂H₂₄
• Molecular Weight: 408.543

Synonyms:4cis.6cis.8cis.2trans-1.2.4.7-Tetraphenyl-cyclooctatetraen

Chemical Property of 4cis.6cis.8cis.2trans-1.2.4.7-Tetraphenyl-cyclooctatetraen

Chemical Property:

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Technology Process of 4cis.6cis.8cis.2trans-1.2.4.7-Tetraphenyl-cyclooctatetraen

There total 8 articles about 4cis.6cis.8cis.2trans-1.2.4.7-Tetraphenyl-cyclooctatetraen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

1,5-Diphenyltricyclo<2.1.0.02,5>pentan-3-on (1146-27-6) → 1,3,5,7-Tetraphenylcyclooctatetraen (35087-43-5) + 1,2,4,7-Tetraphenylcyclooctatetraen (19099-38-8)

Guidance literature:

In dichloromethane; for 2h; Product distribution; Ambient temperature; Irradiation;

Reference yield:

2,4-Bis-(trimethylammonio)-1,3-diphenyl-cyclobutan → 1,2,4,7-Tetraphenylcyclooctatetraen (19099-38-8)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol;

DOI:10.1021/ja01057a033

Reference yield:

C22H32N2(2+)*2I(1-) (39871-87-9) → 1,2,4,7-Tetraphenyl-cyclooctatetraen (19099-38-8)

Guidance literature:

With potassium tert-butylate; (heating);

DOI:10.1021/ja00427a033

upstream raw materials:

1,5-Diphenyltricyclo<2.1.0.0^2,5>pentan-3-on

C₂₂H₃₂N₂⁽²⁺⁾*2I^(1-)

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