Technology Process of C12H6Cl2F3N
There total 5 articles about C12H6Cl2F3N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trichlorophosphate;
for 4h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium carbonate / water; toluene / 20 °C
1.2: 3 h / Heating / reflux
2.1: trichlorophosphate / 5 h / Heating / reflux
3.1: urea hydrogen peroxide adduct; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C
4.1: trichlorophosphate / 4 h / Heating / reflux
With
urea hydrogen peroxide adduct; sodium carbonate; trifluoroacetic anhydride; trichlorophosphate;
In
dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate / 5 h / Heating / reflux
2: urea hydrogen peroxide adduct; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C
3: trichlorophosphate / 4 h / Heating / reflux
With
urea hydrogen peroxide adduct; trifluoroacetic anhydride; trichlorophosphate;
In
dichloromethane;