Li⁽¹⁺⁾*{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}^(1-)*3C₄H₈O=Li{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}*3C₄H₈O

Base Information

• Chemical Name: Li⁽¹⁺⁾*{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}^(1-)*3C₄H₈O=Li{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}*3C₄H₈O
• CAS No.: 89828-36-4
• Molecular Formula: 3C₄H₈O*C₃₃H₂₃Mo₂O₈P₂*Li
• Molecular Weight: 1024.63

Synonyms:Li⁽¹⁺⁾*{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}^(1-)*3C₄H₈O=Li{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}*3C₄H₈O

Chemical Property of Li⁽¹⁺⁾*{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}^(1-)*3C₄H₈O=Li{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}*3C₄H₈O

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Technology Process of Li⁽¹⁺⁾*{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}^(1-)*3C₄H₈O=Li{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}*3C₄H₈O

There total 1 articles about Li⁽¹⁺⁾*{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}^(1-)*3C₄H₈O=Li{(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(O)CH₃)}*3C₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

bis-μ-diphenylphosphido-octacarbonyldimolybdenum (Mo-Mo) + methyllithium (917-54-4) → Li(1+)*{(CO)4Mo(P(C6H5)2)2Mo(CO)3(C(O)CH3)}(1-)*3C4H8O=Li{(CO)4Mo(P(C6H5)2)2Mo(CO)3(C(O)CH3)}*3C4H8O (89828-36-4)

Guidance literature:

In tetrahydrofuran; treating a suspension of 0.38 mmol Mo2(CO)8(μ-P(C6H5)2)2 in THF with 1 equiv of CH3Li (0.39 mmol); stirring for 5 min;; filtration; removing of solvent from the filtrate; elem. anal.;;

DOI:10.1021/ja00246a018

Reference yield:

Li(1+)*Mo2(P(C6H5)2)2(COCH3)(CO)7(1-) = Li[Mo2(P(C6H5)2)2(COCH3)(CO)7] (89828-36-4) + trimethoxonium tetrafluoroborate (420-37-1) → (CO)4Mo(P(C6H5)2)2Mo(CO)3(C(OCH3)CH3) (89828-40-0)

Guidance literature:

In nitromethane; Mo-complex was treated with 1 equiv of Me3OBF4 in MeNO2 for 10 min under N2; product was obtained in poor yield; solvent was removed, product was extd. into THF; formulated from (1)H and (31)P NMR evidence;

upstream raw materials:

methyllithium

Downstream raw materials:

(CO)4Mo(P(C₆H₅)2)2Mo(CO)3(C(OCH₃)CH₃)

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