2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

Base Information

Chemical Name:2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether
CAS No.:223910-46-1
Molecular Formula:C₅₁H₄₄BrN₃O
Molecular Weight:794.834
Hs Code.:

Synonyms:2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

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Chemical Property of 2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

Chemical Property:

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Technology Process of 2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

There total 5 articles about 2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-83-5
trityl chloride

: 223910-46-1
2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / acetonitrile / Ambient temperature

2: 1.) LiAlH₄, 2.) aq. NaOH / 1.) THF, 2.) THF, RT, 15 min

3: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; triethylamine; In acetonitrile;
DOI:10.1021/jm980408v

Reference yield:

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
(R)-histidine methyl ester dihydrochloride

: 223910-46-1
2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / acetonitrile / Ambient temperature

2: 1.) LiAlH₄, 2.) aq. NaOH / 1.) THF, 2.) THF, RT, 15 min

3: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; triethylamine; In acetonitrile;
DOI:10.1021/jm980408v

Reference yield:

: D-Histidine dihydrochloride

: 223910-46-1
2-(R)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-bromobenzyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / SOCl₂ / 60 °C

2: 100 percent / Et₃N / acetonitrile / Ambient temperature

3: 1.) LiAlH₄, 2.) aq. NaOH / 1.) THF, 2.) THF, RT, 15 min

4: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF

With sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; sodium hydride; triethylamine; In acetonitrile;
DOI:10.1021/jm980408v