{2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

Base Information

Chemical Name:{2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester
CAS No.:855529-05-4
Molecular Formula:C₂₅H₃₀N₄O₇
Molecular Weight:498.536
Hs Code.:

{2-[2-(3-<i>tert</i>-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

Synonyms:{2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

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Chemical Property of {2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

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Technology Process of {2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

There total 3 articles about {2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 111331-82-9
3-[(tert-butoxycarbonyl)amino]benzoic acid

: triglycine benzyl ester toluenesulfonic acid salt

: 855529-05-4
{2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

Guidance literature:: 3-[(tert-butoxycarbonyl)amino]benzoic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In chloroform; for 0.5h;

triglycine benzyl ester toluenesulfonic acid salt; With triethylamine; In chloroform; at 20 ℃; for 48h;
DOI:10.1039/b417808b

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 855529-05-4
{2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / aq. KOH / dioxane / 20 h / 20 °C

2.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CHCl₃ / 0.5 h

2.2: 83 percent / Et₃N / CHCl₃ / 48 h / 20 °C

With potassium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; chloroform;
DOI:10.1039/b417808b

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 855529-05-4
{2-[2-(3-tert-butoxycarbonylamino-benzoylamino)-acetylamino]-acetylamino}-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / aq. KOH / dioxane / 20 h / 20 °C

2.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CHCl₃ / 0.5 h

2.2: 83 percent / Et₃N / CHCl₃ / 48 h / 20 °C

With potassium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; chloroform;
DOI:10.1039/b417808b