(1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

Base Information

Chemical Name:(1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate
CAS No.:363583-56-6
Molecular Formula:C₁₈H₂₆OS₂
Molecular Weight:322.536
Hs Code.:

Synonyms:(1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

Suppliers and Price of (1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

There total 1 articles about (1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-15-0,12122-00-8
carbon disulfide

: 104870-80-6
(1R,2R,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexanol

: 77-78-1
dimethyl sulfate

: 363583-56-6
(1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 4h;
DOI:10.1016/S0040-4039(01)01000-0

Reference yield: 90.0%

: 363583-56-6
(1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

: 363583-57-7
(3R,6S)-3-methyl-6-(1-methyl-1-phenylethyl)-1-cyclohexene

Guidance literature:: at 200 ℃; for 1h;
DOI:10.1016/S0040-4039(01)01000-0

Reference yield:

: 363583-56-6
(1R,2R,5R)-S-methyl-O-[5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl]dithiocarbonate

: 100101-42-6
(1S,2R,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 1 h / 200 °C

2: 93 percent / m-CPBA / CH₂Cl₂ / 3 h / 20 °C

3: 98 percent / lithium triethylborohydride / tetrahydrofuran / 20 °C

With lithium triethylborohydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)01000-0