2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 82592-37-8
• Molecular Formula: C₃₂H₃₀N₇P₃
• Molecular Weight: 605.558

Synonyms:2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property:

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Technology Process of 2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 2 articles about 2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (82592-36-7) → 2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (82592-37-8)

Guidance literature:

at 100 ℃; for 3h; under 0.1 Torr;

DOI:10.1139/v82-076

Reference yield:

2,2-dichloro-4,4,6,6-tetraphenyl-cyclotriphosphazene (3606-94-8) → 2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (82592-37-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / trimethylamine / xylene / 192 h / Heating

2: 71 percent / 3 h / 100 °C / 0.1 Torr

With trimethylamine; In xylene;

DOI:10.1139/v82-076

upstream raw materials:

2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

2,2-dichloro-4,4,6,6-tetraphenyl-cyclotriphosphazene

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