Boc-3-OBzl

Base Information

Chemical Name:Boc-3-OBzl
CAS No.:142570-79-4
Molecular Formula:C₅₇H₇₃N₉O₁₅
Molecular Weight:1124.26
Hs Code.:

Synonyms:Boc-3-OBzl

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Chemical Property of Boc-3-OBzl

Chemical Property:

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Technology Process of Boc-3-OBzl

There total 6 articles about Boc-3-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 142570-84-1
Boc-Ala-(BzlO)Gly-Ala-OH

: (S)-2-(2-{[(S)-2-((S)-2-{2-[((S)-2-Amino-propionyl)-benzyloxy-amino]-acetylamino}-propionylamino)-propionyl]-benzyloxy-amino}-acetylamino)-propionic acid benzyl ester; compound with trifluoro-acetic acid

: 142570-79-4
Boc-3-OBzl

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1.) -10 deg C, 2 h, 2.) RT, 24 h;
DOI:10.1246/bcsj.65.1356

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 142570-79-4
Boc-3-OBzl

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran / 0.25 h / -18 °C

2: CH₂Cl₂ / 1.) -18 deg C, 3 h, 2.) 48 h

3: 77 percent / Zn, AcOH / 2.5 h / Ambient temperature

4: 71 percent / Et₃N, HOBt, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide; CH₂Cl₂ / 1.) -10 deg C, 2 h, 2.) RT, 24 h

With benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.65.1356

Reference yield:

: 109208-68-6
Boc-Ala-O-COO-isoBu

: 142570-79-4
Boc-3-OBzl

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 1.) -18 deg C, 3 h, 2.) 48 h

2: 77 percent / Zn, AcOH / 2.5 h / Ambient temperature

3: 71 percent / Et₃N, HOBt, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide; CH₂Cl₂ / 1.) -10 deg C, 2 h, 2.) RT, 24 h

With benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; zinc; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.65.1356