methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Base Information

Chemical Name:methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside
CAS No.:99745-47-8
Molecular Formula:C₂₁H₂₁N₃O₆
Molecular Weight:411.414
Hs Code.:

Synonyms:methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Suppliers and Price of methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

There total 4 articles about methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 99679-79-5
methyl 4,6-O-(phenylmethylene)-2-benzoate-3-(trifluoromethanesulfonate)-α-D-glucopyranoside

: 99745-47-8
methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Guidance literature:: With lithium azide; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 50 ℃; for 4.5h;

Reference yield:

: 28642-64-0,35823-97-3,38992-99-3,51591-23-2,55169-75-0,56253-26-0,72659-78-0,80041-30-1,80299-59-8,86420-70-4,86420-72-6,91685-06-2,99265-94-8,109010-33-5,118246-05-2,126255-07-0
methyl 2-O-benzoyl-4,6-di-O-benzylidene-α-D-glucopyranoside

: 99745-47-8
methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂; pyridine / 5 h / Ambient temperature

2: 68 percent / LiN₃ / dimethylsulfoxide; dimethylformamide / 4.5 h / 50 °C

With lithium azide; In pyridine; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 3162-96-7
4,6-O-benzylidene-1-O-methyl-α-D-glucopyranoside

: 99745-47-8
methyl 3-azido-3-deoxy-4,6-O-(phenylmethylene)-2-benzoate-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: di(n-butyl)tin oxide / methanol

2: pyridine / dichloromethane / 2 h / -20 °C

3: sodium azide; tetrabutyl-ammonium chloride / N,N-dimethyl-formamide / 24 h / 50 °C

With pyridine; sodium azide; tetrabutyl-ammonium chloride; di(n-butyl)tin oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201301112